Overview of Mass Spec Chemical Profiling

What is Mass Spec Chemical Profiling? FIT's new dq1000 "Divining Quad" is a revolutionary new concept in Petroleum Geochemistry and the first commercially available implementation of Mass Spectrometry for on-site, real-time mud gas analysis and logging. Conceptually, the dq1000 is similar to conventional equipment (i.e., hot-wire + GC), in that it continuously analyzes volatiles extracted from the drilling mud and correlates them with depth. But here the similarity ends. At the heart of the dq1000 is a quadrupole mass analyzer which, in addition to performing the usual Total Gas + C1-nC5 analysis, is capable of detecting C6-C13 hydrocarbons (i.e., hexane, heptane, octane, etc.); distinguishing among paraffins, naphthenes and aromatics; and monitoring a variety of water-soluble species such as acetic acid, toluene and benzene, and inorganics including hydrogen, helium, nitrogen, carbon dioxide, oxygen, argon and sulfur-bearing compounds. Correlation of these geochemical indicators with available drilling parameters and lithologic data allow real-time evaluation of Pay, Wetness (e.g., Pixler Ratios), Petroleum Type and Quality, Reservoir Compartmentalization, Fluid Contacts, Seals, etc.

The Divining Quad is a portable, fully-automatic, stand-alone analyzer. Its modest size, weight and electrical requirements facilitate deployment in even the most restrictive environments. Sensor inputs on the dq1000 monitor penetration, circulation, and pump strokes (any of which can also be read from a WITS-enabled local network) to derive Depth, ROP and Lag for the preparation of geochemical logs. While drilling, analytical results may be viewed on-screen locally or remotely and are always available for immediate LAS import into standard logging graphics packages. Bi-directional communication can be enabled over both LAN and the Internet.

The Divining Quad is user friendly requiring minimal instruction for setup, operation and routine maintenance. In field trials, the system has produced continuous, high quality data with minimal operator intervention for months at a time. Unlike FID detectors used in other gas analyzers, no auxiliary gases are needed thereby reducing costs and safety concerns. Mass Spec Analysis eliminates HC/CO2 interference - a common problem with many detectors leading to serious underestimation of hydrocarbons in some cases. The dq1000 accurately distinguishes mud gas from atmosphere allowing automated (and remote) monitoring of gas trap/extraction line performance. Optional two port operation allows evaluation of hydrocarbon recirculation and potential mud additive interference.

Discriminates:

  • C1-C13 Hydrocarbons
  • Paraffins
  • Naphthenes
  • Aromatics
  • Organic Acids
  • Inorganics: CO2, He, N2, O2, H2S, H2, etc.
  • Mud Additives


Real-Time Applications:

  • Pay
  • Petroleum Type
  • Compartmentalization
  • Fluid Contacts
  • Seals


DQ1000 Wellsite Chemical Profiler Specifications:

  • Dimensions: 26in x 7.5in x 15in
  • Weight: 61 lb (Portable)
  • Power: 85-264 VAC (3.0-1.5 Amp); 47-63 Hz (International)
  • Network: LAN and Internet Enabled
  • Sensors: Depth, Circulation, Pump Strokes (3)
  • Cycle Time: ~15sec - 6min (2 min. nominal)
  • Analysis: Dual (differential) or Single Port Gas Stream

 

Updated 01/09/06